MétaCan
Menu
Back to cohort
Record W4247652853 · doi:10.1002/047084289x.rl121.pub2

Lithium Iodide

2006· reference-entry· en· W4247652853 on OpenAlexaff
André B. Charette, J. Kent Barbay, Wei He

Bibliographic record

VenueEncyclopedia of Reagents for Organic Synthesis · 2006
Typereference-entry
Languageen
FieldChemistry
TopicCoordination Chemistry and Organometallics
Canadian institutionsUniversité de Montréal
Fundersnot available
KeywordsAnhydrousChemistryIodideAcetoneIodineNuclear chemistryLithium iodideSolubilityLithium chlorideHydrateLithium (medication)HydrideDiethyl etherInorganic chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

[10377-51-2] ILi (MW 133.84) InChI = 1S/HI.Li/h1H;/q;+1/p-1 InChIKey = HSZCZNFXUDYRKD-UHFFFAOYSA-M (ester cleavage and decarboxylation;2 source of nucleophilic iodide;3 mild Lewis acid;1 salt effects in organometallic reactions;1 epoxide opening4) Physical Data: mp 449 °C; bp 1180 °C; d 4.076 g cm−3. Solubility: 165 g/100 mL H2O (20 °C); 433 g/100 mL H2O (80 °C); 251 g/100 mL EtOH (20 °C); 343 g/100 mL MeOH (20 °C); 43 g/100 mL acetone (18 °C); very sol NH4OH. Form Supplied in: anhydrous white solid or as the hydrate. Preparative Method: the anhydrous salt of high purity can be prepared from lithium hydride and iodine in ether.5 Purification: crystallized from hot H2O (0.5 mL g−1) by cooling in CaCl2–ice or from acetone. LiI is dried for 2 h at 120 °C (0.1 mmHg, P2O5) before use. Handling, Storage, and Precautions: for best results, LiI should be dried prior to use in anhydrous reactions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Other · Consensus signal: Other
Teacher disagreement score0.195
Threshold uncertainty score0.653

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0020.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0020.002
Science and technology studies0.0010.000
Scholarly communication0.0010.001
Open science0.0030.002
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.1950.192

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.237
Teacher spread0.223 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designNot applicable
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2006
Admission routes1
Has abstractyes

Explore more

Same venueEncyclopedia of Reagents for Organic SynthesisSame topicCoordination Chemistry and OrganometallicsFrench-language works237,207