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Record W4249731864 · doi:10.26434/chemrxiv.12912452

Folding in Place: Design of β-Strap Motifs to Stabilize the Folding of Hairpins with Long Loops

2020· preprint· en· W4249731864 on OpenAlexfundno aff
Alexis D. Richaud, Guangkuan Zhao, Stéphane P. Roche, Samir Hobloss

Bibliographic record

VenueChemRxiv · 2020
Typepreprint
Languageen
FieldEngineering
TopicAdvanced Materials and Mechanics
Canadian institutionsnot available
FundersNational Institutes of HealthNational Institute of General Medical SciencesMitacs
KeywordsChemistryStereochemistryProtein foldingCrystallographyBiophysicsBiologyBiochemistry

Abstract

fetched live from OpenAlex

Despite their pivotal role in protein function and antibody binding affinity, <i>β</i>-hairpins bearing long non-canonical loops are a challenge to modern synthesis because of the large entropic penalty associated with their folding. Little is known about the contribution and impact of stabilizing motifs on the folding of <i>β</i>-hairpins of variable length and plasticity. Here we report a direct comparison between these <i>b</i>-straps thermodynamics and their thermal stability behavior using several local spectroscopic probes of the folding/unfolding landscape. The judicious cooperative interactions crafted in <i>β</i>-Strap <u>R</u>W(<u>V</u>W)•••(W<u>V</u>/<u>H</u>)W<u>E</u> (<i>strap</i> = <i>str</i>and + c<i>ap</i>) greatly stabilized hairpins with up to 10-residue loops lacking an innate nucleating-turn locus (<i>T<sub>m</sub> </i>up to 52 <sup>o</sup>C; 88 ± 1% folded at 291 K). The present design of novel <i>β</i>-straps aims to provide the foundation to study new classes of long hairpins and ultimately offer an attractive alternative to macrocyclic peptides for the mimicry of functional loops from proteins and antibodies.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.617
Threshold uncertainty score0.929

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.033
GPT teacher head0.238
Teacher spread0.205 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2020
Admission routes1
Has abstractyes

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