Formation of Inter-Diffusion Layer between NiCrAlY Coating and Nb Substrate during Vacuum Heat-Treatment
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Bibliographic record
Abstract
The formation of the inter-diffusion layer between NiCrAlY coating and Nb substrate during vacuum heat treatment was investigated. A NiCrAlY coating was applied on Nb substrate by cathode arc deposition. Vacuum heat treatments were carried out at 800, 900, and 1000°C for 2 h. SEM, EPMA, EDS, and XRD were performed to analyze the microstructure of the inter-diffusion layer and the results were interpreted using the 1002°C isothermal ternary Nb-Ni-Cr phase diagram. It was found that at 800°C the inter-diffusion layer has a single NbNi3 layer; at 900°C the inter-diffusion layer consists of an outer NbNi3 layer, a thin intermediate NbCr2(HT) layer, and an inner Nb7Ni6 layer; at 1000°C the inter-diffusion layer has three well-developed layers of an outer NbNi3 layer, an inner Nb7Ni6 layer, and an intermediate layers comprising NbCr2(HT) and NbNi3. A small amount of Cr exists in both the NbNi3 and the Nb7Ni6 phases as solid solution, and a large amount of Ni in the NbCr2(HT) phase as solid solution.
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Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
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Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it