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Record W4296071474 · doi:10.1016/j.mfglet.2022.07.046

Manufacturing of Pitch Based Carbon Fibers through Microwave Treatments

2022· article· en· W4296071474 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueManufacturing Letters · 2022
Typearticle
Languageen
FieldEngineering
TopicFiber-reinforced polymer composites
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsMaterials scienceCarbonizationComposite materialUltimate tensile strengthThermal treatmentFourier transform infrared spectroscopyModulusCarbon fibersMicrowaveMesophaseThermalSpecific modulusElastic modulusComposite numberChemical engineeringScanning electron microscope

Abstract

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Carbon fibers (CFs) are characterized by their excellent mechanical properties including high tensile strength and elastic modulus. In terms of manufacturing of CFs, the conventional thermal treatment processes, including stabilization and carbonization, account for at least 46% of the cost, which drastically restricts the widespread application of CFs. This study investigates the use of mesophase pitch-based CFs from different synthetic approaches based on the conventional thermal post-treatment versus microwave hybrid post-treatment processes. CFs were studied by using SEM, FTIR, TGA, XRD, and mechanical properties characterization. Compared with the CFs prepared from the conventional thermal post-treatment process (CFs-T), those by the microwave thermal hybrid post-treatment process (CFs-M) show similar crystalline degree which is confirmed by XRD analysis. The tensile strength and modulus of the CFs-T are 0.290 and 38.6 GPa, and those of the CFs-M are 0.176 and 18.5 GPa, respectively. Microwave treatment is expected to be a much more energy- and time-efficient way for CFs post-treatment and can serve as a potential alternative to the conventional thermal post-treatment process used in carbon fiber manufacturing. Implications of the findings, including the oxygen diffusion, and crystalline structure are highlighted and discussed.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.663
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.180
Teacher spread0.173 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it