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Record W4321443541 · doi:10.1002/cpz1.696

Multiplex Quantification of Plasma Biomarkers for Patients with Gaucher Disease Type 1

2023· article· en· W4321443541 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueCurrent Protocols · 2023
Typearticle
Languageen
FieldMedicine
TopicLysosomal Storage Disorders Research
Canadian institutionsCentre Intégré Universitaire de Santé et de Services Sociaux du Centre-Sud-de-l'Île-de-MontréalUniversité de Sherbrooke
Fundersnot available
KeywordsGlucocerebrosidaseChromatographyChemistryMultiplexHigh-performance liquid chromatographySphingolipidMedicineEnzymeBiochemistryBioinformaticsBiology

Abstract

fetched live from OpenAlex

Abstract Gaucher disease (GD) is a lysosomal storage disorder caused by a deficiency of the enzyme beta‐glucocerebrosidase. This leads to the accumulation of glycolipids in macrophages and ultimately results in tissue damage. Recent metabolomic studies highlighted several potential biomarkers in plasma specimens. In hopes of better understanding the distribution, importance, and clinical significance of these potential markers, a UPLC‐MS/MS method was developed and validated to quantify lyso‐Gb 1 and six related analogs (with the following modifications on the sphingosine moiety: ‐C 2 H 4 (‐28 Da), ‐C 2 H 4 +O (‐12 Da), ‐H 2 (‐2 Da), ‐H 2 +O (+14 Da), +O (+16 Da), and +H 2 O (+18 Da)), sphingosylphosphorylcholine, and N‐ palmitoyl‐O‐phosphocholineserine in plasma specimens of treated and untreated patients. This 12‐min UPLC‐MS/MS method involves a purification step via solid‐phase extraction followed by evaporation under nitrogen flow and resuspension in an organic mix compatible with HILIC chromatography. This method is currently used for research purposes and might be used for monitoring, prognostics, and follow‐up. © 2023 The Authors. Current Protocols published by Wiley Periodicals LLC.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: Observational
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.060
Threshold uncertainty score0.331

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.114
GPT teacher head0.415
Teacher spread0.301 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it