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Vesicular Nanostructures Prepared by Reactive Melt Blending We are grateful to the Services Fédéraux des Affaires Scientifiques, Techniques et Culturelles for general support in the frame of “PAI 4-11: Supramolecular Chemistry and Supramolecular Catalysis”. We are grateful to Sunil K. Varshney (Polymer Source Inc., Canada) for training and advice in anionic polymerization and to Mrs. Martine Dejeneffe for ultramicrotomy at low temperature. Dr. Koen Janssen and Mai Quaedflieg from DSM Research (Geleen, The Netherlands) are acknowledged for making the mini-extruder available to us. C.K. is a Research Fellow of the “Fonds National de la Recherche Scienctifique” (FNRS, Belgium).

2002· article· en· W4324013320 on OpenAlexaboutno aff
Christian Koulic, Zhihui Yin, Christophe Pagnoulle, Robert Jérôme

Bibliographic record

VenueAngewandte Chemie International Edition · 2002
Typearticle
Languageen
FieldChemistry
TopicAdvanced Polymer Synthesis and Characterization
Canadian institutionsnot available
Fundersnot available
KeywordsSubstructurePolyamideCopolymerMaterials scienceTransmission electron microscopyMorphology (biology)PolystyrenePolymer chemistryPolymer scienceNanostructureChemical engineeringComposite materialPolymerNanotechnologyBiologyZoology

Abstract

fetched live from OpenAlex

A three-layer substructure morphology is found in the vesicular nanostructures formed (see transmission electron micrograph) upon melt blending of polyamide 12 (PA12) with a symmetric polystyrene-b-polyisoprene (PS-b-PIP) copolymer end-capped by an anhydride group. However, macrophase separation occurs when the diblock is unreactive.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.012
Threshold uncertainty score0.588

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.052
GPT teacher head0.338
Teacher spread0.286 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations10
Published2002
Admission routes1
Has abstractyes

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