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Record W4372318944 · doi:10.1021/acsanm.3c00771

Graphdiyne Quantum Dots for H<sub>2</sub>O<sub>2</sub> and Dopamine Detection

2023· article· en· W4372318944 on OpenAlexafffund
Syed Rahin Ahmed, Ana Gomez Cardoso, Herlys Viltres Cobas, Poushali Das, Aicheng Chen, Seshasai Srinivasan, Amin Reza Rajabzadeh

Bibliographic record

VenueACS Applied Nano Materials · 2023
Typearticle
Languageen
FieldMaterials Science
TopicAdvanced Nanomaterials in Catalysis
Canadian institutionsUniversity of GuelphMcMaster University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsFluorescenceQuantum dotDetection limitX-ray photoelectron spectroscopyBiosensorMaterials scienceUltravioletChemistryPhotochemistryAnalytical Chemistry (journal)NanotechnologyChemical engineeringOrganic chemistryChromatographyOptoelectronics

Abstract

fetched live from OpenAlex

The fluorescence and nanozymatic nature of quantum dots (QDs) in a single entity provide an excellent opportunity for the development of sensitive fluorescence and colorimetric biosensing and bioimaging approaches. Herein, the hydrothermal synthesis method of fluorescent graphdiyne quantum dots (GDY QDs) from graphdiyne sheets is presented. This research reports, for the first time, the nanozymatic activity of GDY QDs besides their conventional fluorescent nature, which catalyzes the oxidation of H 2 O 2 through the peroxidase biomimetic nature and enables detection of H 2 O 2 and dopamine. The peaks of the ultraviolet–visible (UV–vis) spectrum and the fluorescence emission of GDY QDs are located at 395 and 450 nm, respectively. The X-ray photoelectron spectroscopic (XPS) results reveal that GDY and GDY QDs have similar carbon skeletons. Moreover, the intensity of C–O and C═O peaks in GDY QDs is stronger than that of GDY, suggesting the successful surface oxidation of GDY, which is crucial for hydrophilicity and catalytic activity. Kinetic analysis reveals that as-synthesized GDY QDs exhibit Michaelis–Menten kinetic behavior. The terephthalic acid and DPPH test confirms the hydroxyl radical formation and scavenging nature of GDY QDs, playing a significant role in enhancing the nanozymatic activity. The biomimetic nature of GDY QDs is applied for H 2 O 2 and dopamine detection, and limit of detection (LOD) values of 0.13 and 8.65 μM are obtained for H 2 O 2 and dopamine, respectively. The findings of this study will open a door to the development of carbon-based nanocrystals with an enzyme-mimicking nature that can lead to the development of analytical approaches, in particular, colorimetric nanobiosensors.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.241
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations49
Published2023
Admission routes2
Has abstractyes

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