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Record W4376106276 · doi:10.1111/jace.19184

Resolved‐detrimental surface crystallization in yttrium lanthanum gallate glasses for optical fiber applications

2023· article· en· W4376106276 on OpenAlexaff
Florian Calzavara, Pierre Florian, Franck Fayon, Vincent Sarou‐Kanian, Théo Guérineau, Sylvain Danto, Younès Messaddeq, Marc Dussauze, Véronique Jubera, Thierry Cardinal, Evelyne Fargin

Bibliographic record

VenueJournal of the American Ceramic Society · 2023
Typearticle
Languageen
FieldMaterials Science
TopicGlass properties and applications
Canadian institutionsUniversité LavalInstitut National d'Optique
FundersUniversité de BordeauxCentre National de la Recherche ScientifiqueAgence Nationale de la Recherche
KeywordsYttriumMaterials scienceDevitrificationCrystallizationLanthanumGallateMineralogyOxideChemical engineeringInorganic chemistryMetallurgyChemistryNuclear chemistry

Abstract

fetched live from OpenAlex

Abstract Gallium‐rich heavy metal oxide glasses have become highly attractive optical materials since they exhibit a wide transparency window spanning from the ultraviolet ∼270 nm up to the mid‐infrared (IR) region ∼6 μm making them promising for a future integration in optical fiber devices. Nonetheless, in most composition, surface crystallization is a key limiting factor for optical fiber drawing using the classical preform‐to‐fiber method. Herein, taking advantage of structural information from vibrational spectroscopies (Raman/IR) and 71 Ga Solid‐State Nuclear Magnetic Resonance, we describe the key role of lanthanum and yttrium rare—earth elements on the glass structure and their impact on the capability to draw those new glass compositions into optical fibers. This approach emphasizes that yttrium ions as compared with lanthanum ones favor the glass disorder, increasing significantly the fraction of GaO 5 units with respect to GaO 4 . That, combined with thermal analysis and examination of the crystallization behaviors, highlights that Y 2 O 3 prevents the glass devitrification during the glass shaping. The smaller yttrium radius is believed to be the key physical parameter preventing the precipitation of the Ba y Ga 5‐y Ge y+1 La 3‐y O 14 ( y = 0, 1, 2, 3) langasite‐type crystal phase. This study remains particularly relevant and opens up the way for the development of highly robust power scaled fiber devices operating from the visible up to the challenging mid‐IR domain.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.466
Threshold uncertainty score0.274

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.284
Teacher spread0.264 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2023
Admission routes1
Has abstractyes

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Same venueJournal of the American Ceramic SocietySame topicGlass properties and applicationsFrench-language works237,207