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Record W4385706597 · doi:10.3749/2200050

Discreditation of <i>Borishanskiite</i> as a Mineral Species (= Polarite, PdPb)

2023· article· en· W4385706597 on OpenAlexaff
Louis J. Cabri, Andrew M. McDonald, Tatiana L. Evstigneeva

Bibliographic record

VenueThe Canadian Journal of Mineralogy and Petrology · 2023
Typearticle
Languageen
FieldChemistry
TopicChemical Thermodynamics and Molecular Structure
Canadian institutionsLaurentian University
Fundersnot available
KeywordsChemistryStructural formulaCrystallographyMoleculeMineralOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract A re-examination by electron probe microanalysis of the holotype sample of the platinum-group mineral borishanskiite, previously defined as Pd1+x(As,Pb)2 with x = 0–0.2, reveals that the mineral contains no detectable As. The new data also show the mineral to be stoichiometric, i.e., vacancy-free, with the average chemical composition (based on 2 apfu) of Pd0.99(Pb0.72Bi0.28)Σ1.00 (n = 3) or ideally, PdPb. A comparison of the powder X-ray diffraction patterns for borishanskiite (PDF 00-029-0960) and polarite (PDF 00-023; ideally PdPb) show that, within error, the two are same. Further, the refined unit-cell parameters of borishanskiite, a = 7.18(2), b = 8.62(2), c = 10.66(2) Å, agree well with those of polarite, a = 7.140, b = 8.563, c =10.501 Å. Given the new chemical data for borishanskiite, which suggest the ideal chemical formula PdPb, along with its crystallographic similarity to polarite, it is concluded that borishanskiite is equivalent to polarite. Discussion of the extent of the PdBi–PdPb solid-solution series and confusion concerning the ideal formula for polarite is also presented.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.915
Threshold uncertainty score0.994

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.214
Teacher spread0.206 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2023
Admission routes1
Has abstractyes

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