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Coprocessing Partially Hydrodeoxygenated Hydrothermal Liquefaction Biocrude from Forest Residue in the Vacuum Gas Oil Hydrocracking Process

2023· article· en· W4386085767 on OpenAlexafffund
Sandeep Badoga, Anton Alvarez‐Majmutov, Julie Katerine Rodriguez, Rafał Gieleciak, Jinwen Chen

Bibliographic record

VenueEnergy & Fuels · 2023
Typearticle
Languageen
FieldEngineering
TopicThermochemical Biomass Conversion Processes
Canadian institutionsNatural Resources Canada
FundersCanadian Forest ServiceOffice of Energy Research and Development
KeywordsHydrothermal liquefactionHydrodesulfurizationNaphthaVacuum distillationChemistryDistillationHydrodenitrogenationDiesel fuelFluid catalytic crackingPulp and paper industryCrackingChemical engineeringOrganic chemistryCatalysis

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Hydrodeoxygenation of biogenic feedstocks is an option to alleviate the challenges associated with their coprocessing in petroleum refinery units. This study investigates the effect of coprocessing a partially hydrodeoxygenated biocrude with vacuum gas oil (VGO) in a hydrocracking process. The biocrude, produced by hydrothermal liquefaction (HTL) of forest residues, was hydrodeoxygenated to an oxygen level of 3.6 wt % at which it became fully miscible in the VGO feed. The coprocessing feed blend was constituted of 7.5 wt % hydrodeoxygenated biocrude in 92.5 wt % VGO. Pilot plant tests were carried out in two sequential stages: hydrotreating and hydrocracking. Hydrotreating was performed first, with the purpose of meeting the sulfur and nitrogen specifications of the hydrocracking catalyst. The hydrotreated products next underwent hydrocracking to produce enough product for physical distillation. The tests were conducted using pure VGO first to set a baseline for the study and then the coprocessing feed. During both hydrotreating and hydrocracking, coprocessing required increasing the reactor temperature by 10–15 °C over the baseline temperature for pure VGO to offset the poisoning effect of oxygen compounds. The hydrotreating stage was also affected by reactor plugging issues attributed to unstable high-boiling material in the biocrude. In spite of this, the coprocessing scheme was shown to stand on par with the VGO baseline in terms of overall product distribution and without consuming more hydrogen. Moreover, the coprocessed naphtha, diesel, and jet fuel fractions showed only subtle differences in properties and hydrocarbon composition relative to those from VGO. Biogenic carbon measurements revealed that the coprocessed naphtha, diesel, and jet fuel fractions contained 8–9 wt % biogenic carbon.

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How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.010
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.223
Teacher spread0.212 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations10
Published2023
Admission routes2
Has abstractyes

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