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Radiation Tolerance of Lead Halide Perovskite Films: An <i>in Situ</i> X-ray Scattering Study

2023· article· en· W4388465528 on OpenAlex
Renita M. D’Souza, Timothy L. Kelly

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Materials Letters · 2023
Typearticle
Languageen
FieldEngineering
TopicPerovskite Materials and Applications
Canadian institutionsUniversity of Saskatchewan
FundersNatural Sciences and Engineering Research Council of CanadaUniversity of Saskatchewan
KeywordsPerovskite (structure)HalideMaterials scienceOptoelectronicsRadiationRadiation damageIrradiationScatteringIonizing radiationOpticsChemistryPhysicsCrystallographyInorganic chemistry

Abstract

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Lead halide perovskites, known for their excellent optoelectronic properties, have found application in solar cells, LEDs, and photodetectors. One particularly promising application of these materials is in X-ray detectors. This requires a high degree of tolerance to the effects of ionizing radiation, and one of the main drawbacks of lead halide perovskites is their instability, with respect to a wide variety of environmental stimuli. Although we know a lot about how moisture, oxygen, and visible light affect and degrade the perovskite lattice, relatively little is known about the radiation tolerance of these materials. In this work, we discuss the effect of high-energy (15.12 keV) X-ray radiation on perovskites of various compositions. We use in situ GIWAXS (grazing incidence wide-angle X-ray scattering) to follow the structural changes that occur as the result of X-ray exposure in atmospheres of varying relative humidity. Perhaps surprisingly, we find that there is a low compositional and humidity dependence on the rate of radiation damage in perovskite films. An accumulating radiation dose is associated with increasing structural disorder including the formation of ion vacancies and Schottky defects. These results are an important first step in the design of robust, radiation-tolerant, and perovskite-based X-ray detectors.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.092
Threshold uncertainty score0.873

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.236
Teacher spread0.223 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it