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Record W4390746927 · doi:10.1021/acs.chemmater.3c01391

Nanocomposite Aerogel Network Featuring High Surface Area and Superinsulation Properties

2024· article· en· W4390746927 on OpenAlexaff
Solmaz Karamikamkar, Abdelnasser Abidli, Omid Aghababaei Tafreshi, Shahriar Ghaffari‐Mosanenzadeh, Piyapong Buahom, Hani E. Naguib, Chul B. Park

Bibliographic record

VenueChemistry of Materials · 2024
Typearticle
Languageen
FieldChemistry
TopicAerogels and thermal insulation
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsAerogelMaterials scienceThermoplastic polyurethaneNanocompositeComposite materialThermal decompositionComposite numberNanofiberPorosityChemical engineeringElastomerOrganic chemistry

Abstract

fetched live from OpenAlex

A nanocomposite strategy for the combination of a polymerized silica precursor, such as polyvinyltrimethoxysilane (P-VTMS), together with electrospun thermoplastic polyurethane (TPU) nanofiber in the aerogel backbone is demonstrated to create effective stress transfer pathways in three-dimensional (3-D) aerogel composites with thermal insulation characteristics and special porous structure. Inspired by the bone architecture in the human body, with large amounts of hard segments and small amounts of soft segments, the 3-D interconnected TPU-embedded P-VTMS-based composite (P-VTMS/TPU) aerogel achieves synergistic strengthening in the nanofiber orientation direction. The sol–gel approach followed by first spinodal decomposition and later binodal decomposition phase separation has been taken in this study to initiate network formation throughout the P-VTMS/TPU backbone to form a 3-D network porous structure. The structure obtained offers full hierarchical multimodal porosity and an unprecedentedly large surface area of 2146 m 2 g –1 due to a special approach taken in the sol–gel process in designing the interface between electrospun TPU nanofibers and P-VTMS chains. Owing to the combination of excellent mechanical and thermal insulation properties, the P-VTMS/TPU composite aerogel can be used as a thermal insulation material. Such a hierarchical multimodal porous architecture opens the door to fabricating new 3-D multifunctional and mechanically durable nanocomposite aerogels for flexible devices.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.205
Teacher spread0.189 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations35
Published2024
Admission routes1
Has abstractyes

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