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FA<sub>4</sub>Pb<sub>2</sub>I<sub>7.5</sub>(SCN)<sub>0.5</sub>: <i>n</i> = 3 Member of Perovskite Homologous Series FA<sub><i>n</i>+1</sub>Pb<sub><i>n</i>−1</sub>I<sub>3<i>n</i>−1.5</sub>(SCN)<sub>0.5</sub> with Columnar Defects

2024· article· en· W4394881461 on OpenAlex
Takuya Ohmi, James R. Neilson, Wataru Taniguchi, Teppei Nagase, Yuki Haruta, Makhsud I. Saidaminov, Takanori Fukushima, Masaki Azuma, Takafumi Yamamoto

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueACS Materials Letters · 2024
Typearticle
Languageen
FieldEngineering
TopicPerovskite Materials and Applications
Canadian institutionsUniversity of Victoria
FundersJapan Society for the Promotion of ScienceOffice of ScienceMinistry of Education, Culture, Sports, Science and Technology
KeywordsHomologous seriesThiocyanatePerovskite (structure)PhotoluminescenceHalideCrystallographyMaterials scienceLattice (music)Series (stratigraphy)Band gapIonChemistryInorganic chemistryOptoelectronicsPhysics

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Hybrid organic–inorganic halide perovskites are an emerging class of optoelectronic materials. Among them, there are many homologous series of Ruddlesden–Popper and Dion–Jacobson layered perovskites reported, but a homologous series based on defect ordering has not yet been discovered. Here, by using thiocyanate anion as a defect generator, we successfully synthesized a new defect-ordered perovskite FA 4 Pb 2 I 7.5 (SCN) 0.5 together with the previously reported FA 6 Pb 4 I 13.5 (SCN) 0.5 . These compounds can be represented respectively as n = 3 and n = 5 members of the perovskite homologous series FA n +1 Pb n −1 I 3 n −1.5 (SCN) 0.5 with ordered columnar defects, which is the first homologous series of defect-ordered hybrid perovskites. The optical band gap increases with an increase in the ordered defects in the lattice. FA 4 Pb 2 I 7.5 (SCN) 0.5 ( n = 3) exhibits photoluminescence emission, which is a feature of layered perovskites with a quantum-well structure. This study provides a new strategy to control the defect orderings for tuning their optical properties by incorporating thiocyanate.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.005
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Scholarly communication, Open science, Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Science and technology studies, Research integrity
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.032
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0050.001
Meta-epidemiology (narrow)0.0100.011
Meta-epidemiology (broad)0.0100.004
Bibliometrics0.0040.007
Science and technology studies0.0030.004
Scholarly communication0.0060.006
Open science0.0060.004
Research integrity0.0050.005
Insufficient payload (model declined to judge)0.0000.005

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.190
Teacher spread0.183 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it