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Record W4399162747 · doi:10.1002/adma.202406094

Thiosalicylic‐Acid‐Mediated Coordination Structure of Nickel Center via Thermodynamic Modulation for Aqueous Ni–Zn Batteries

2024· article· en· W4399162747 on OpenAlex
Yichun Su, Guoqiang Yuan, Jinliang Hu, Guangxun Zhang, Yijian Tang, Yihao Chen, Yiluo Tian, Shuli Wang, Mohsen Shakouri, Huan Pang

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueAdvanced Materials · 2024
Typearticle
Languageen
FieldEngineering
TopicAdvanced battery technologies research
Canadian institutionsCanadian Light Source (Canada)University of Saskatchewan
FundersYangzhou UniversityGovernment of Jiangsu ProvinceNatural Science Foundation of Jiangsu ProvinceNational Natural Science Foundation of China
KeywordsMaterials scienceNanomaterialsNickelDensity functional theoryElectrochemistryLigand (biochemistry)MoleculeX-ray photoelectron spectroscopyNanotechnologyPhysical chemistryChemical engineeringComputational chemistryElectrodeChemistryMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Uniquely functional nanocomplexes with rich coordination environments are critical in energy storage. However, the construction of structurally versatile nanocomplexes remains challenging. In this study, a nickel‐based complex with structural variations is designed via thermodynamic modulation using a dual‐ligand synthesis strategy. A nickel‐based nanomaterial (NiSA‐SSA‐160) with a large specific surface area is synthesized around the competing coordination of the host and guest molecules that differ in terms of the chemical properties of the O and S elements. Concurrently, the coordination environment of NiSA‐SSA‐160 is investigated via X‐ray absorption fine structure spectroscopy. The thiol functional groups synergistically induced an electron‐rich Ni structure, thus increasing the electron density of the central atom. The electrochemical performance of an assembled NiSA‐SSA‐160//Zn@CC battery is shown to improve significantly, with a maximum energy density of 0.54 mWh cm −2 and a peak power density of 49.49 mW cm −2 . This study provides a new perspective regarding coordination transformations and offers an idea for the design of functionally rich nanomaterials.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.098
Threshold uncertainty score0.914

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.260
Teacher spread0.253 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it