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Effect of Pressure on Visbreaking Product Composition and Properties

2024· article· en· W4400278830 on OpenAlexafffund
Priscila T. H. Nascimento, Arno de Klerk

Bibliographic record

VenueEnergy & Fuels · 2024
Typearticle
Languageen
FieldChemistry
TopicPetroleum Processing and Analysis
Canadian institutionsUniversity of Alberta
FundersNatural Sciences and Engineering Research Council of CanadaAlberta InnovatesChina National Offshore Oil Corporation
KeywordsComposition (language)Process engineeringProduct (mathematics)ChemistryMathematicsEngineering

Abstract

fetched live from OpenAlex

Visbreaking is a thermal conversion process employed to decrease the viscosity of residual oils, and cracking occurs mainly in the liquid phase. The impact of pressure on thermal cracking is expected to be minor, yet several observations in the literature indicate that pressure may affect coking, the olefin-to-paraffin ratio, and product composition. In this study, the impact of pressure on coil visbreaking at 400 °C was evaluated in a closed system at a severity sufficient to cause the onset of coking. The products from thermal conversion with initial pressures of 0.5–2.0 MPa (low pressure) differed from those with initial pressures of 2.5–4.0 MPa (high pressure). High pressure suppressed coking, and at comparable vacuum residue conversion, the coke yield was lower at high pressure than at low pressure. Pressure had a minor impact on the distillation profile of the products. Under conditions of controlled space time, pressure did not affect the olefin-to-paraffin ratio, H/C molar ratio, or microcarbon residue. Pressure had an impact on composition-dependent properties, such as the first derivative of density and refractive index with respect to temperature, viscosity, and aromatic hydrogen content. No relationship was found between initial pressure and free radicals, n -pentane insoluble content, and molar element ratios measured in the study.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.007

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.226
Teacher spread0.219 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations4
Published2024
Admission routes2
Has abstractyes

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