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Record W4402916488 · doi:10.1002/chem.202403458

Platinum‐Centered Oligoynes Capped by Boron Difluoride Formazanate Dyes and Their Thin‐Film Properties

2024· article· en· W4402916488 on OpenAlexafffund
Erin L. Cotterill, Tiago Carneiro Gomes, Amélie C. P. Teare, Yasmeen Jaberi, Jasveer S. Dhindsa, Paul D. Boyle, Simon Rondeau‐Gagné, Joe B. Gilroy

Bibliographic record

VenueChemistry - A European Journal · 2024
Typearticle
Languageen
FieldChemistry
TopicSynthesis and Properties of Aromatic Compounds
Canadian institutionsUniversity of WindsorWestern University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsAlkyneMaterials scienceMicroscale chemistryConductivityCarbyneNanotechnologyConjugated systemSemiconductorPlatinumPolyacetyleneThin filmChemical engineeringPolymer chemistryPolymerChemistryOrganic chemistryOptoelectronicsPhysical chemistryComposite material

Abstract

fetched live from OpenAlex

Abstract Since the Nobel prize winning discovery that polyacetylene could act as a semiconductor, there has been tremendous efforts dedicated to understanding and harnessing the unusual properties of π‐conjugated polymers. Much of this research has focused on the preparation of oligoynes and polyynes with well‐defined numbers of repeating alkyne units as models for carbyne. These studies are usually hampered by a structure‐property relationship where the stability of the resulting materials decrease with the incorporation of additional alkyne units. Here, we describe a series of oligoynes, with up to 12 alkyne units, where electron‐rich [Pt(PBu 3 ) 2 ] 2+ units are incorporated at the center of the oligoyne backbones which are capped by electron‐poor BF 2 formazanate dyes. These compounds exhibit excellent stability and solubility, panchromatic absorption, and redox activity characteristic of their structural components. These traits facilitated thin‐film studies of extended oligoyne materials, where it is shown that incorporating [Pt(PBu 3 ) 2 ] 2+ units leads to smoother films, decreased conductivity on the microscale, and increased conductivity on the nanoscale when compared to metal‐free analogs. Remarkably, our oligoynes have superior conductivity compared to the ubiquitous poly(3‐hexylthiophene) semiconductor.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.149
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.193
Teacher spread0.177 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2024
Admission routes2
Has abstractyes

Explore more

Same venueChemistry - A European JournalSame topicSynthesis and Properties of Aromatic CompoundsFrench-language works237,207