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Record W4404219805 · doi:10.1002/cjce.25544

A study on the adequacy of some actinides adsorption on a modified guanidine Schiff base from laboratory effluents

2024· article· en· W4404219805 on OpenAlexvenueno aff
Sabreen M. El‐Gamasy, Amal E. Mubark, Samar Ebrahim Abd-El Razek, Ahmed A. Eliwa

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2024
Typearticle
Languageen
FieldChemistry
TopicRadioactive element chemistry and processing
Canadian institutionsnot available
Fundersnot available
KeywordsGuanidineSchiff baseActinideChemistryNuclear chemistryAdsorptionEffluentRadiochemistryWaste managementOrganic chemistryPolymer chemistryEngineering

Abstract

fetched live from OpenAlex

Abstract Besides the distinctive features and medicinal benefits of guanidine Schiff bases, the possibility of their use as a sorbent for radioactive contents of effluents was developed in the current study. A series of adsorption experiments were performed with 2,2‐benzene‐1,4‐dildiguanidine di‐salicylate synthesized sorbent from sulphate feed solutions containing UO 2 2+ and ThSO 4 2+ species each separately. Infrared studies demonstrated that the sorbent links to both actinides via the azomethine nitrogen atom and the hydroxyl groups on the sorbent. Thermal analyses were also performed. Using the greatest adsorption results, UO 2 2+ and ThSO 4 2+ were able to bind to modified guanidine Schiff base (MGSB) sorbent with uptake capacities of 98 and 54 mg/g respectively. The maximal uptake was achieved at pH 5.5 and 3.5 and 90 min contact time for UO 2 2+ and ThSO 4 2+ , respectively. The equilibrium adsorption results for UO 2 2+ and ThSO 4 2+ were in good agreement with Langmuir isotherm and the pseudo‐second‐order reaction model and demonstrated the endothermic nature and kinetic improvement by increasing temperatures. All kinetic and isotherm results demonstrated the chemical adsorption of both UO 2 2+ and ThSO 4 2+ at the MGSB active sites. Positive ∆ H (40.54 and 40.16 kJ/mol for UO 2 2+ and ThSO 4 2+ , respectively) proved the endothermic nature of the adsorption process.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.467

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.238
Teacher spread0.216 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2024
Admission routes1
Has abstractyes

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