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Record W4405307989 · doi:10.1101/2024.12.10.627789

Development of a <i>De Novo</i> Protein Binder that Inhibits the Alpha Kinase eEF2K

2024· preprint· en· W4405307989 on OpenAlexafffund
Kody A. Klupt, Ethan Belrose, Zongchao Jia

Bibliographic record

VenuebioRxiv (Cold Spring Harbor Laboratory) · 2024
Typepreprint
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicATP Synthase and ATPases Research
Canadian institutionsQueen's University
FundersNatural Sciences and Engineering Research Council of CanadaQueen's University
KeywordsAlpha (finance)ChemistryCell biologyMolecular biologyBiologyMedicineSurgery

Abstract

fetched live from OpenAlex

SUMMARY Elongation factor 2 kinase (eEF2K) is calmodulin activated and phosphorylates eEF2, a GTPase, that regulates global translation. When eEF2K phosphorylates eEF2, protein translation is halted. This process may be critical to studying how diseases like cancer dysregulate protein synthesis. eEF2K is an alpha kinase and not targeted by conventional kinase inhibitors. Traditional methods of structure-based drug design are incredibly time consuming and expensive, which may involve screening large libraries of small molecules. We have generated de novo small binder proteins (∼10kDa) - using RFDiffusion and ProteinMPNN. One promising de novo binder protein we produced, ‘CAM1’ binds to a hydrophobic patch on the calmodulin binding domain of eEF2K with nanomolar affinity as determined by isothermal titration calorimetry. This binder, in vitro , significantly reduces eEF2 peptide phosphorylation, comparable to the gold-standard small molecule eEF2K inhibitor, A-484954. The predicted structure of CAM1 is a helical bundle which has been confirmed by circular dichroism spectroscopy. Impressively, CAM1 has a melting temperature >80 0 C, and is produced recombinantly in bacteria, greater than 5 mg / culture liter. We have also determined that CAM1 transfection significantly reduces mammalian HeLa cell proliferation comparable to A-484954 treatment and inhibits the phosphorylation of eEF2. Our de novo binder, the first to our knowledge to inhibit an alpha kinase, and the first non-competitive eEF2K inhibitor, establishes an alternative method of targeting atypical kinase activity.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Methods · Consensus signal: none
Teacher disagreement score0.001
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.254
Teacher spread0.234 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2024
Admission routes2
Has abstractyes

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