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Record W4405987635 · doi:10.1101/2025.01.01.631036

Discrimination between <i>Mycobacterium tuberculosis</i> and <i>Mycobacterium bovis</i> using Fourier Transform Infrared Spectroscopy

2025· preprint· en· W4405987635 on OpenAlexaff
Kevim Bordignon Guterres, Taiana Tainá Silva‐Pereira, Rodrigo Juliano Oliveira, Carolyn G. J. Moonen, Marcos Bryan Heinemann, Flábio R. Araújo, Moisés Palaci, Ana M. S. Guimarães

Bibliographic record

VenuebioRxiv (Cold Spring Harbor Laboratory) · 2025
Typepreprint
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicSpectroscopy Techniques in Biomedical and Chemical Research
Canadian institutionsWiLAN (Canada)
Fundersnot available
KeywordsMycobacterium bovisMycobacterium tuberculosisTuberculosisMycobacteriumMicrobiologyBiologyMycobacterium tuberculosis complexVirologyMedicinePathology

Abstract

fetched live from OpenAlex

ABSTRACT Zoonotic tuberculosis (TB) caused by Mycobacterium bovis (Mb) is a neglected disease that hinders efforts to eradicate human tuberculosis. Developing a rapid, high-throughput diagnostic test to distinguish Mb from Mycobacterium tuberculosis (Mtb) isolates could enhance global zoonotic TB diagnostics and surveillance. This study aimed to evaluate the ability of Fourier Transform Infrared Spectroscopy (FT-IRS), using the IR Biotyper® system, to differentiate clinical isolates of Mb and Mtb. Two bacterial inactivation protocols— paraformaldehyde and boiling—were tested using Mtb and BCG strains grown in liquid culture. While both methods allowed FT-IRS analysis, boiling was preferred due to its ease of use and efficiency in biomass recovery. Subsequently, Mtb and Mb isolates were analyzed using FT-IRS, and the resulting spectra were used to construct a sample classifier employing machine learning algorithms. Linear Discriminant Analysis (LDA) and a UPGMA dendrogram demonstrated clear separations between Mtb and Mb ecotypes. Additionally, a classifier built and internally validated using artificial neural networks achieved 99% accuracy in distinguishing Mb and Mtb. Further FT-IRS analysis of few available Mycobacterium africanum (Maf) strains demonstrated its capacity to differentiate Maf from Mtb and Mb, expanding its utility in regions where Maf is endemic. This is the first study to apply FT-IRS to distinguish tuberculous mycobacteria. FT-IRS proved to be a highly effective, rapid, and accurate diagnostic tool for differentiating Mb and Mtb strains, with promising applications for other tuberculous mycobacteria such as Maf. IMPORTANCE Zoonotic tuberculosis (TB) caused by Mycobacterium bovis (Mb) remains a major threat due to its clinical similarity to human TB, higher rates of extrapulmonary cases, and resistance to pyrazinamide, complicating treatment. Current diagnostic methods used to differentiate M. tuberculosis (Mtb) from Mb and are limited by costs, resource needs, and technical complexity. We developed a method based on Fourier Transform Infrared Spectroscopy (FT-IRS) to differentiate Mb and Mtb clinical isolates with high accuracy. This diagnostic assay offers advantages over traditional molecular techniques by eliminating the need for DNA extraction, requiring less technical expertise, and providing fast, accurate differentiation of Mtb and Mb strains. This innovative approach can improve global diagnostics and surveillance of zoonotic TB.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.273
Teacher spread0.261 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes1
Has abstractyes

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