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Record W4407800889 · doi:10.1002/wer.70047

Quantifying and characterizing major DOC fractions in water treatment processes: A simplified SPE method without recovering sorbed compounds

2025· article· en· W4407800889 on OpenAlexafffund
Saeideh Mirzaei, Beata Gorczyca

Bibliographic record

VenueWater Environment Research · 2025
Typearticle
Languageen
FieldEnvironmental Science
TopicWater Treatment and Disinfection
Canadian institutionsUniversity of Manitoba
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsFractionationDissolved organic carbonChemistryTrihalomethaneWater treatmentEnvironmental chemistryExtraction (chemistry)Fraction (chemistry)ChromatographySolid phase extractionEnvironmental engineeringOrganic chemistryEnvironmental science

Abstract

fetched live from OpenAlex

absorption (SUVA) as an indicator of hydrophobic (HPO) dissolved organic carbon (DOC) to evaluate removal efficiency and estimate trihalomethane formation potential (THMFP). However, current fractionation methods, such as solid-phase extraction (SPE), primarily focus on recovering sorbed compounds, and assume that treatment impacts only the quantity, not the characteristics, of DOC fractions. Additionally, varying recovery rates and inconsistent fractionation pH definitions complicate cross-study comparisons of hydrophilic and HPO DOC composition. To address these issues, we tested three pH fractionation approaches (pH 3, pH 7, and sequential adjustment) and observed significant differences in DOC content, SUVA, and specific THMFP (STHMFP) between SPE filtrates at pH 3 and pH 7, which were most likely because of ionizable acidic DOC compounds becoming HPO at lower pH levels. Based on these findings, we developed a new fractionation method to estimate the quantity and characteristics of major DOC fractions-hydrophilic neutral (HPIN), total acidic (TA = HPOA + HPIA), and hydrophobic neutral (HPON)-without the need to recover sorbed fractions. Applying this method in a conventional coagulation/softening plant revealed HPON decreased while the relative amounts of HPI and TA increased after the treatment. However, the treated water HPI exhibited significantly higher STHMFP and contained approximately twice the proportion of low-molecular-weight compounds than raw water HPI, highlighting significant changes in both the content and properties of DOC fractions throughout the treatment process. Our study indicates that the contribution of HPI DOC fraction to SUVA and STHMFP in treated water is greater than that of HPO DOC. PRACTITIONER POINTS: A two-stage ENV to estimate major DOC fractions without recovering sorbed compounds. One ENV cartridge at pH 3 can effectively isolate HPI DOC, replacing sequential ENV. Coagulation and lime/soda softening altered characteristics of DOC fractions. HPI DOC in treated water contributes to SUVA and STHMFP more than HPO fraction.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.239
Threshold uncertainty score0.975

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.072
GPT teacher head0.366
Teacher spread0.294 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes2
Has abstractyes

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