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Record W4409672987 · doi:10.1002/pro.70114

Optimization of synthetic human <scp>V<sub>H</sub></scp> affinity and solubility through in vitro affinity maturation and minimal camelization

2025· article· en· W4409672987 on OpenAlexafffund
Kasandra Bélanger, Cunle Wu, Traian Sulea, Henk van Faassen, Deborah Callaghan, Annie Aubry, Marc Sasseville, Greg Hussack, Jamshid Tanha

Bibliographic record

VenueProtein Science · 2025
Typearticle
Languageen
FieldMedicine
TopicMonoclonal and Polyclonal Antibodies Research
Canadian institutionsUniversity of OttawaNational Research Council Canada
FundersPacific Northwest National LaboratoryNational Research Council Canada
KeywordsThermostabilityAffinity maturationPhage displayImmunogenicitySolubilityIn vitroChemistryAffinity chromatographyAntigenMutantBiochemistrySaturated mutagenesisMutagenesisStereochemistryCombinatorial chemistryBiologyPeptideEnzymeGeneticsGene

Abstract

fetched live from OpenAlex

Abstract An attractive feature of human V H s over camelid V H Hs as immunotherapeutics is their perceived lower risk of immunogenicity. While human V H s can readily be obtained from synthetic phage display libraries, they often suffer from low affinity and poor solubility compared to V H Hs derived from immune libraries. Using SARS‐CoV‐2 spike protein as a model antigen, we screened a synthetic human V H phage display library and identified a diverse set of antigen‐specific V H s. However, the V H s exhibited low affinity, and many had low solubility; that is, they were prone to aggregation. To explore the feasibility of improving the affinity, we subjected a representative V H to in vitro affinity maturation. We created a yeast surface display library of V H variants employing a site‐saturated mutagenesis approach targeting complementarity‐determining regions and selected against the target antigen. Next‐generation sequencing of the selected variants, combined with structural modeling, identified a set of V H s as potentially improved candidates. Characterization of these candidates revealed several V H s with improved affinities of up to 100‐fold ( K D s as low as 3 nM) and potent neutralization capabilities; however, they still showed significant aggregation. By introducing as few as two camelid residues into the framework region 2 of a high‐affinity V H (a process referred to as camelization), we were able to completely solubilize the V H without compromising its affinity and other important attributes, including thermostability and protein A binding. This study demonstrates the feasibility of generating high‐affinity, ‐solubility, and ‐stability human V H s from synthetic libraries through a combination of in vitro affinity maturation and minimal camelization.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.108
Threshold uncertainty score0.389

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.309
Teacher spread0.288 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2025
Admission routes2
Has abstractyes

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