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Record W4410242876 · doi:10.1021/acsami.5c02907

The Influence of Nickel and Alkali Metal Additives on Manganese Dioxide Structure and Performance for Rechargeable Zinc-Ion Batteries

2025· article· en· W4410242876 on OpenAlexafffund
Storm Gourley, Caio M. Miliante, Alejandra Ibarra-Espinoza, Thomas James Baker, Navid Noor, Oleg Rubel, Brian D. Adams, Drew Higgins

Bibliographic record

VenueACS Applied Materials & Interfaces · 2025
Typearticle
Languageen
FieldEngineering
TopicAdvanced battery technologies research
Canadian institutionsMcMaster University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsMaterials scienceManganeseNickelAlkali metalZincInorganic chemistryAlkaline batteryMetalChemical engineeringMetallurgyElectrodeElectrolyteOrganic chemistryChemistry

Abstract

fetched live from OpenAlex

Aqueous rechargeable zinc-ion batteries (ZIBs) are a promising addition to the energy storage landscape, particularly supporting the decarbonization of the power sector (i.e., deployment of wind and solar) as a low-cost, high-safety alternative to lithium-ion batteries. Unfortunately, wide-scale ZIB utilization is hindered in part by limited energy storage capacity and operational durability of state-of-the-art Mn oxide cathode materials. As such, we take a combined approach to investigate the impact of simultaneous inclusion of alkali metal (Li, Na, K, Rb, and Cs) and Ni additives on the structural and electrochemical properties of Mn oxide-based cathode materials for ZIBs. We used a facile, scalable synthesis approach to prepare 15 unique Mn oxide-based cathode materials and identified several materials capable of delivering a practical rate (i.e., C/10) discharge capacity of >150 mAh g –1 and a fast charge (i.e., 1C) capacity retention of >90% after 200 cycles. Detailed characterization of the prepared materials revealed the use of alkali metal additives during synthesis impacted both phase structure and electrochemical performance. Modifying the phase structure of Mn oxides resulted in an elevated Zn 2+ diffusion coefficient for K-containing materials and a subsequent increase in deliverable capacity. Furthermore, the incorporation of Ni in the structure was shown to have no meaningful contribution to improved capacity within the aqueous electrolyte stability window, although a slight uptick in capacity retention was observed for all prepared materials as Ni content was increased. Considering the narrow range of reported cathodes for ZIBs, this work provides insight on the important interplay between structure, composition, and improved performance of Mn oxide-based cathodes, helping accelerate future material development efforts necessary for ZIB commercialization.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.525

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.246
Teacher spread0.237 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2025
Admission routes2
Has abstractyes

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