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Record W4411527947 · doi:10.1002/cjce.70004

Thermal degradation of impact‐modified <scp>PMMA</scp> in mechanical and chemical recycling

2025· article· en· W4411527947 on OpenAlexaffvenue
Nguyen Tien Dat, Nooshin Saadatkhah, Yanfa Zhuang, Jacopo De Tommaso, Karen Stoeffler, Adrien Faye, Gregory S. Patience

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2025
Typearticle
Languageen
FieldMaterials Science
TopicPolymer crystallization and properties
Canadian institutionsNational Research Council CanadaPolytechnique Montréal
Fundersnot available
KeywordsMaterials scienceDepolymerizationMethyl methacrylateComposite materialUltimate tensile strengthPyrolysisPoly(methyl methacrylate)ThermoplasticIzod impact strength testInjection mouldingPolymerChemical engineeringMonomerPolymer chemistry

Abstract

fetched live from OpenAlex

Abstract Poly (methyl methacrylate) (PMMA) is a thermoplastic with outstanding tensile strength, UV resistance, and a high level of transparency that has been used widely for optical applications such as glazing in the automobile industry. Mechanical recycling, the most widespread method, degrades the physical properties and prevents reusing PMMA in transparent applications. Thermal depolymerization to recover methyl methacrylate (MMA) monomer is becoming an alternative route for PMMA recycling. In this paper, the thermal depolymerization process of impact‐modified PMMA in a micro fluidized bed reactor was investigated. The pyrolysis was conducted over aluminium oxide () and fluid‐cracking catalyst (FCC) as catalytic beds; sand and SiC as inert beds at temperatures below . A mechanical recycling process was also simulated using sequential injection moulding to investigate its impact on the properties of PMMA. After 5 cycles of injection moulding, the impact strength and optical properties of PMMA were severely diminished due to an increase in free volume and partial thermal degradation. Regarding PMMA pyrolysis, demonstrated limited cracking ability with a maximum MMA yield of 46%, as opposed to FCC, which over‐cracked both PMMA and MMA into coke and unwanted products. In contrast, non‐catalytic beds exhibited higher activity for MMA recovery, with SiC yielding the highest amount of 92% at .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score0.237

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.215
Teacher spread0.202 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2025
Admission routes2
Has abstractyes

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