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Influence of bainitic transformation temperature on microstructure evolution during isothermal holding and subsequent cooling

2025· article· en· W4412079776 on OpenAlexafffund
Ehsan Tolouei, Mohammad Saadati, Jean-Benoît Morin, Carlos García-Mateo, Mohammad Jahazi

Bibliographic record

VenueMaterials Chemistry and Physics · 2025
Typearticle
Languageen
FieldEngineering
TopicMicrostructure and Mechanical Properties of Steels
Canadian institutionsCégep de Sorel-TracyÉcole de Technologie Supérieure
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsIsothermal processMicrostructureTransformation (genetics)Materials scienceThermodynamicsContinuous cooling transformationSlow coolingIsothermal transformation diagramMetallurgyChemistryBainitePhysics

Abstract

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Modified mold steels have recently gained attention as a novel approach in steel grades due to their high-performance applications. In this study, high-resolution dilatometry was used to study the isothermal bainitic transformation of a medium-carbon low-alloy steel after full austenitization at 900 ˚C, followed by austempering for 3 hours at temperatures ranging from 380 to 450 ˚C. The results showed that no bainitic phase transformation occurred at 450 ˚C, while an incomplete transformation was observed at all lower tested temperatures, and martensitic transformation occurred upon cooling at the final stage. Increasing the austempering temperature from 380 ˚C to 425 ˚C resulted in a lower volume fraction of bainite and a higher amount of martensite, whereas at 450 ˚C, a full lath martensite microstructure formed during final cooling. Electron backscatter diffraction (EBSD) and scanning electron microscopy (SEM) analyses revealed that increasing the isothermal holding temperature led to increased thickness of the bainitic blocks and a higher volume fraction of martensite. Vickers hardness increased from 412 to 500 HV between 380 and 450 ˚C holding temperatures. This increase was attributed to the phase volume fraction, the carbon content of martensite, and the thickness of bainitic ferrite blocks. Nanoindentation tests were conducted on different martensitic and bainitic regions to compare the influence of isothermal holding temperature on the characteristics of the phases. The results indicated that as the isothermal temperature increased, the carbon content of martensite decreased, leading to a reduction in the nanohardness of the martensitic regions from 8.3 GPa at 400 ˚C to 7.8 GPa at 425 ˚C and 6.9 GPa at 450 ˚C. Furthermore, the average block thickness of bainitic ferrite increased from 0.71 μm to 1.98 μm as the isothermal temperature was raised from 380 ˚C to 425 ˚C, resulting in a decrease in nanohardness from 6.3 to 5.4 GPa. These findings are interpreted in terms of the evolution of bainitic block thickness and the carbon content of martensite at different austempering temperatures, as well as their impact on the hardness of the phases.

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How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.010

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.003
GPT teacher head0.180
Teacher spread0.177 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations0
Published2025
Admission routes2
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