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Record W4412530406 · doi:10.1016/j.mineng.2025.109631

Separation of rare earth elements via pickering emulsion: A sustainable approach to physicochemical beneficiation

2025· article· en· W4412530406 on OpenAlexafffund
Mohammed Zriki, Adrián Carrillo García, Louis Fradette, Jamal Chaouki

Bibliographic record

VenueMinerals Engineering · 2025
Typearticle
Languageen
FieldEngineering
TopicExtraction and Separation Processes
Canadian institutionsPolytechnique Montréal
FundersOCP GroupMitacs
KeywordsBeneficiationPickering emulsionEmulsionRare earthEarth (classical element)Chemical engineeringChemistryMaterials scienceEngineeringMetallurgyPhysics

Abstract

fetched live from OpenAlex

Separating rare earth elements (REE) bearing minerals from their associated gangue minerals, such as dolomite and calcite, is challenging, particularly for fine particle size, due to their similar physicochemical surface properties. To exploit the small differences in surface properties between the gangue and the REE minerals, a solid stabilized emulsification (SSE) process was developed to concentrate the fine REE minerals, bastnaesite, and monazite, from carbonate minerals. Our study examines the minerals’ surface properties, contact angle, and zeta potential, on the resulting mineral-oil–water emulsion systems. The mineral separation occurred naturally, without surface modifiers, using key operating parameters, like moderate agitation (450 rpm), low oil viscosity (< 20 cSt), and a pH ranging from 6 to 10. In the fine ore (< 38 µm), REE-bearing minerals, predominantly liberated or highly exposed, had a strong affinity for the oil phase (contact angle > 59°), compared to the carbonate minerals (contact angle < 48°), which remained in the aqueous phase. As monazite and bastnaesite, particularly monazite, tended to attach to the oil, a 68 % REE recovery and an enrichment ratio of 2.9 occurred in a single-stage emulsification process. This study showcases SSE as a promising sustainable solution for rare earth beneficiation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.000
Threshold uncertainty score0.001

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.241
Teacher spread0.234 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2025
Admission routes2
Has abstractyes

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