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Automatic NMR Spectral Profiling of Commercial Cow’s Milk

2025· article· en· W4413003132 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Food Science & Technology · 2025
Typearticle
Languageen
FieldChemistry
TopicSpectroscopy and Chemometric Analyses
Canadian institutionsThe Metabolomics Innovation CentreUniversity of Alberta
FundersAlberta InnovatesCanada Foundation for InnovationNational Center for Complementary and Integrative HealthGenome Canada
KeywordsProfiling (computer programming)ChemistryComputer scienceOperating system

Abstract

fetched live from OpenAlex

MagMet is a program capable of automatically processing and profiling one-dimensional (1D) 1 H NMR spectra of complex mixtures of small molecules. We have previously adapted MagMet for the automated analysis of human biofluids, including filtered serum and fecal extracts as well as beverages such as wine and beer. In this study, we have developed a new version of MagMet (MagMet-M) capable of profiling the 1D 1 H NMR spectra of commercial cow’s milk acquired at 700 MHz. This version of MagMet contains a library of 81 abundant, small molecule metabolites commonly detected in commercial cow’s milk samples. MagMet-M was optimized to accurately identify and quantify these metabolites in four types of commercial cow’s milk with varying milk fat content. The performance of the automated profiling by MagMet-M was evaluated by comparison to manual profiling using the commercial software Chenomx (version 8.3). Good agreement was observed between the two programs, with overall median and mean absolute percent error of 5 and 9%, respectively. Furthermore, automated analysis by MagMet-M is more than ten times faster than manual analysis, making MagMet-M suitable for high throughput applications. MagMet is available at https://www.magmet.ca .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.077
Threshold uncertainty score0.591

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.007
Science and technology studies0.0000.002
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.297
Teacher spread0.282 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it