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Record W4413243113 · doi:10.1016/j.jcis.2025.138658

Liquid–liquid encapsulation with a constrained interfacial layer

2025· article· en· W4413243113 on OpenAlexafffund
Sirshendu Misra, Akash Chowdhury, Sushanta K. Mitra

Bibliographic record

VenueJournal of Colloid and Interface Science · 2025
Typearticle
Languageen
FieldEngineering
TopicInnovative Microfluidic and Catalytic Techniques Innovation
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaUniversity of Waterloo
KeywordsEncapsulation (networking)Chemical engineeringLiquid liquidMaterials scienceChemistryChromatographyComputer science

Abstract

fetched live from OpenAlex

HYPOTHESIS: Liquid-liquid encapsulation enables rapid wrapping of liquid core droplets using liquid interfacial layer(s) floating on a host liquid bath, but is conventionally limited to shell-forming liquids lighter than the host bath and suffers from uncontrolled lateral spreading of the interfacial layer. We hypothesize that introducing a simple hydrophobic loop at the air-host liquid interface will (i) anchor denser interfacial liquids by interfacial pinning, circumventing the density constraint, and (ii) confine lateral spread, allowing thicker films to form from the same volume of the interfacial layer and improving process control. EXPERIMENTS: Encapsulation experiments were performed using two hydrophobic loops placed one at a time at the surface of deionized water or surfactant-laden aqueous baths. Shell-forming liquids included silicone oils and dibutyl phthalate. Top and side view imaging characterized lens formation with and without the loop. Core droplets were released from controlled heights to vary the impact Weber number, and dynamics were captured using high-speed imaging. A regime map was constructed for three cases: no loop and two loops with different dimensions. Minimum and maximum effective volumes were identified for each loop. FINDINGS: The hydrophobic loop enabled stable confinement of denser interfacial liquids and produced visibly thicker lenses. The trapping-to-penetration transition boundary shifted upward with confinement, more strongly for smaller loops. Each loop exhibited a finite operable volume window. The thicker confined layers also reduced air entrapment by prolonging the residence time of the core droplet. Despite differences in geometry, the two loops showed similar transition Weber numbers at overflow, suggesting geometric similarity at the overflow limit. Overall, the loop enhances shell-liquid utilization, reduces air inclusion, and extends the versatility of liquid-liquid encapsulation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.257
Teacher spread0.250 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes2
Has abstractyes

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