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Record W4413243580 · doi:10.1016/j.ijms.2025.117507

Hydrogenating atomic coinage metal cations (group 11) with H2 on charged He droplets (T<10 K) doped with metal Atoms: Early stages, ligation energies, core structures, group variations, and relativistic effects

2025· article· en· W4413243580 on OpenAlexaff
Olga V. Lushchikova, Milan Ončák, J. Reichegger, B. Felsner, Diethard K. Böhme, P. Scheier

Bibliographic record

VenueInternational Journal of Mass Spectrometry · 2025
Typearticle
Languageen
FieldPhysics and Astronomy
TopicQuantum, superfluid, helium dynamics
Canadian institutionsYork University
FundersUniversität InnsbruckStandortagentur TirolAustrian Science Fund
KeywordsChemistryGroup (periodic table)MetalDopingPlatinum groupAtomic physicsAnalytical Chemistry (journal)Inorganic chemistryOrganic chemistryPlatinumCatalysisCondensed matter physics

Abstract

fetched live from OpenAlex

Experimental mass-spectrometric results are reported which demonstrate that ionized helium nanodroplets (at T < 10 K) doped with the coinage metal atoms M = Cu, Ag or Au, and then exposed to molecular hydrogen, provide an abundance of singly and multiply hydrogenated coinage metal cations M + (H 2 ) n and MH + (H 2 ) n with n up to 25 and beyond. We explore here the information provided by observed distributions in the measured intensities of these ligated ions with n = 1–6 and use ab initio quantum chemical calculations to extract fundamental insights into variations in ligation energies and structures with increasing H 2 ligation and going down the Periodic Table (M + = Cu + , Ag + and Au + ) with an eye on the role of relativistic contributions to the ligation energies expected with the increasing nuclear charge of M + . “Magic” numbers of H 2 additions with relatively high intensity are apparent among the first 5, especially the first 2, H 2 additions. Very substantial relativistic enhancements of the third over the second-row ligation energies were computed, especially for Au + : 83 % and 60 % respectively, for the first two H 2 ligands intimately bonded to Au + , and 19 % and 67 % respectively, for the addition of the first two H 2 ligands to AuH + . Relativistic enhancements for the addition of a third H 2 ligand and beyond were found to be essentially negligible. • Charged He nano-droplets doped with coinage metal M atoms yield H 2 ligated M + and MH + . • “Magic” numbers of H 2 additions of relatively high intensity are seen among the first 5. • Calculations provide core structures for M + (H 2 ) n and MH + (H 2 ) n with n = 1 to 6. • Calculated ligation energies show variations down the Group with second-row minima. • Calculated H 2 ligation energies increase for Au + and AuH + due to relativistic effects.

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How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Theoretical or conceptual · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.664
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.228
Teacher spread0.224 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designTheoretical or conceptual
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes1
Has abstractyes

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