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Record W4413808671 · doi:10.1021/acs.jmedchem.5c01584

Hit-to-Lead Optimization of Acetazolamide-Based Bacterial Carbonic Anhydrase Inhibitors with Efficacy In Vivo for Treatment of Vancomycin-Resistant Enterococci Septicemia

2025· article· en· W4413808671 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of Medicinal Chemistry · 2025
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicEnzyme function and inhibition
Canadian institutionsPurdue Pharma (Canada)
FundersHorizon 2020 Framework ProgrammeNational Institute of Allergy and Infectious DiseasesMinistero dell’Istruzione, dell’Università e della RicercaPurdue Institute for Drug DiscoveryPurdue University
KeywordsChemistryAcetazolamideIn vivoCarbonic anhydraseVancomycinMicrobiologyAntibioticsEnterococcusVancomycin-Resistant EnterococciPharmacologyEnzymeBacteriaBiochemistryStaphylococcus aureusInternal medicineMedicineBiology

Abstract

fetched live from OpenAlex

As one of the leading causes of hospital-acquired infections reported by the National Healthcare Safety Network, vancomycin-resistant enterococci (VRE) continue to afflict patients in healthcare facilities, with limited FDA-approved drugs available for treating systemic infections. Our group previously showed the 1,3,4-thiadiazole acetazolamide human carbonic anhydrase inhibitor scaffold can be repositioned with potent in vitro efficacy against enterococcal pathogens. However, only acetazolamide has been explored for in vivo efficacy in murine septicemia models. Herein, we report a hit-to-lead account in which we expand the structure–activity relationship for the 1,3,4-thiadiazole scaffold, identified lead candidates with favorable in vitro ADME profiles, and advanced a promising lead analog forward into in vivo pharmacokinetic studies. Ultimately, we demonstrated efficacy in a murine septicemic peritonitis infection model after oral dosing. Overall, we demonstrate a successful example of an acetazolamide-based lead compound with in vivo therapeutic potential for the treatment of septicemic vancomycin-resistant VRE infection.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.461

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.250
Teacher spread0.244 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it