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Defining the sources and evolution of nitrate in coal mine rock with stable isotopes of nitrate and ammonium

2025· article· en· W4414825582 on OpenAlexafffund
M. Jim Hendry, Erin E. Schmeling

Bibliographic record

VenueApplied Geochemistry · 2025
Typearticle
Languageen
FieldEnvironmental Science
TopicMethane Hydrates and Related Phenomena
Canadian institutionsUniversity of Saskatchewan
FundersUniversity of Saskatchewan
KeywordsNitrificationNitrateAmmoniumCoal miningNitrogenAmmonium nitrate

Abstract

fetched live from OpenAlex

Elevated concentrations of nitrate (NO 3 ˉ) are present in many surface waters associated with coal mining throughout the world. Its presence is generally attributed to blasting using ANFO (NH 4 NO 3 and fuel oil) to access the coal. A recent study conducted by our group shows the nitrification of naturally occurring exchangeable ammonium (NH 4 + -ex) in waste rock can be a major source of NO 3 − compared to contributions from NO 3 − and the nitrification of NH 4 + originating from blast products. Here we show that neither the concentrations of nitrogen species nor the δ 15 N-NO 3 − and δ 15 N-NH 4 + values can be used to differentiate the sources of NO 3 − . However, the measured δ 18 O-NO 3 ˉ values of NH 4 NO 3 (+24.3±1.7 ‰) and NO 3 ˉ produced from nitrification of both sources of NH 4 + (-4.7 ‰) under oxic laboratory conditions enabled the distinction between these two sources of NO 3 ˉ. Fitting the results of a simple mixing model to the experimental data allowed the concentrations of NO 3 ˉ derived from NH 4 NO 3 in fresh-blasted mine rock to be estimated. The results of this study show the application of δ 18 O-NO 3 ˉ is a valuable technique to characterize the source(s) and evolution of NO 3 − draining from mine rock piles. • Nitrate in mine rock is often attributed to blasting using ammonium nitrate • Nitrification of geogenic ammonium is major source of nitrate in coal mine rock • The nitrogen-15 isotopes cannot be used to differentiate the sources of nitrate. • Oxygen-18 isotopes of nitrate can be used to differentiate between sources of nitrate • Nitrate concentrations from potential sources can be estimated using a mixing model

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.304
Threshold uncertainty score0.247

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.003
GPT teacher head0.176
Teacher spread0.174 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes2
Has abstractyes

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