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Combining proteolytic enzyme with non-thermal ultrasound and microwave methods for enhanced extractability and modified functionality of dry bean (Phaseolus vulgaris) starch: A chemical-free strategy

2025· article· en· W4415387284 on OpenAlexafffund
Prudhvi Pasumarthi, Annamalai Manickavasagan

Bibliographic record

VenueInternational Journal of Biological Macromolecules · 2025
Typearticle
Languageen
FieldNursing
TopicFood composition and properties
Canadian institutionsUniversity of Guelph
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsStarchAmyloseExtraction (chemistry)Retrogradation (starch)Mung beanUltrasoundSwellingMicrowaveProteolytic enzymes

Abstract

fetched live from OpenAlex

This study investigated the extraction of dry bean starch using a food-grade protease enzyme and its integration with ultrasound and microwave treatments, to compare their effects on starch recovery and functional properties. Enzymatic treatment at 0.5 % protease concentration yielded a starch recovery comparable to the conventional alkaline method (∼ 84 %). Integration with ultrasound and microwave allowed higher recovery (∼ 87 %) at lower enzyme concentrations of 0.1 % and 0.25 %, respectively. Ultrasound treatment significantly modified starch characteristics, including surface damage, amylose content, thermal stability, retrogradation behavior, swelling power, solubility, pasting viscosities, rheological properties, and crystallinity. In contrast, microwave treatment induced limited changes, mainly enhancing gel strength and pasting properties while reducing crystallinity. In vitro digestibility revealed monophasic behavior, with ultrasound-treated starch exhibiting increased digestibility and a higher expected glycemic index (eGI). Thus, protease-assisted extraction offers a sustainable alternative to alkaline methods, while its integration with ultrasound or microwave reduces enzyme requirements, enhances starch recovery, and alters starch functionality, yielding application-specific starch without additional modification.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.000
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.036
GPT teacher head0.332
Teacher spread0.296 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2025
Admission routes2
Has abstractyes

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