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Record W4415714890 · doi:10.1016/j.jspr.2025.102861

Influence of moisture content and sub-zero storage conditions on thermogram behaviour of canola seeds

2025· article· en· W4415714890 on OpenAlexafffund
Abhinav Tiwari, Fuji Jian

Bibliographic record

VenueJournal of Stored Products Research · 2025
Typearticle
Languageen
FieldAgricultural and Biological Sciences
TopicFood Drying and Modeling
Canadian institutionsUniversity of Manitoba
FundersNatural Sciences and Engineering Research Council of CanadaCanada Foundation for InnovationResearch Manitoba
KeywordsCanolaDifferential scanning calorimetryMoistureEnthalpyWater contentFreezing pointCongelationMelting point

Abstract

fetched live from OpenAlex

Wet, oil-rich seeds such as canola are especially prone to freeze-induced viability loss under sub-zero temperatures (<0 °C) during handling, processing, and storage. This study characterized the thermogram parameters of canola seeds with different moisture contents (MC, wet basis, 4.% - 30%) under low and sub-zero temperatures (5, -5, -15, and -25 °C). Both frozen canola seeds (20.1% MC stored at -25 °C for more than 20 wks before DSC test) and fresh seeds (different MC and not frozen before DSC test) were tested. Thermogram transitions were largely moisture dependant. Freezing events were not detected in canola seeds with <12% MC. This reflects the biological state of water that at low MC, water is predominantly bound and does not crystallize. Distinct exothermic freezing events occurred at ≥14% MC, signifying detectable freezable water and ice formation. Notably, cooling rate and cooling temperature did not influence the nucleation and freezing point temperature. The freezing point temperature of canola seeds with ≥ 14% MC was about -2.5 to -8 °C. Modulated differential scanning calorimetry showed canola oil components contributed freezing events at around -30 °C, involving significant enthalpy changes. A significant reduction in melting enthalpy was found in frozen seeds compared to fresh seeds, indicating cell structure damage. This study provides crucial mechanistic understanding, advancing cold-climate preservation strategies for canola and offering broader insights for other oilseeds and grains. • First thermal evidence of freeze thresholds in stored canola across wide MC range. • Ice nucleation initiated above 14% MC; critical for sub-zero seed storage. • MDSC revealed enthalpy loss at -25 °C, indicating structural collapse. • Seeds ≤12% MC showed no freezing, validating existence of critical MC threshold. • Reveals limited impact of cooling rate on ice nucleation in low MC canola seeds.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.843
Threshold uncertainty score0.177

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.082
GPT teacher head0.331
Teacher spread0.248 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes2
Has abstractyes

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