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Record W6921850024 · doi:10.1021/es500131k.s001

Profiling\nOil Sands Mixtures from Industrial Developments\nand Natural Groundwaters for Source Identification

2014· article· en· W6921850024 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

aboutThe title or abstract carries a Canadian signal from the geographic lexicon.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueFigshare · 2014
Typearticle
Languageen
FieldSocial Sciences
TopicEducation Methods and Technologies
Canadian institutionsnot available
Fundersnot available
KeywordsGroundwaterTailingsOil sandsMass spectrometryNatural (archaeology)High resolutionNaphthenic acidElectrospray ionization

Abstract

fetched live from OpenAlex

The\nobjective of this study was to identify chemical components\nthat could distinguish chemical mixtures in oil sands process-affected\nwater (OSPW) that had potentially migrated to groundwater in the oil\nsands development area of northern Alberta, Canada. In the first part\nof the study, OSPW samples from two different tailings ponds and a\nbroad range of natural groundwater samples were assessed with historically\nemployed techniques as Level-1 analyses, including geochemistry, total\nconcentrations of naphthenic acids (NAs) and synchronous fluorescence spectroscopy (SFS).\nWhile these analyses did not allow for reliable source differentiation,\nthey did identify samples containing significant concentrations of\noil sands acid-extractable organics (AEOs). In applying Level-2 profiling\nanalyses using electrospray ionization high resolution mass spectrometry (ESI-HRMS)\nand comprehensive multidimensional gas chromatography time-of-flight\nmass spectrometry (GC × GC-TOF/MS) to samples containing appreciable\nAEO concentrations, differentiation of natural from OSPW sources was\napparent through measurements of O<sub>2</sub>:O<sub>4</sub> ion class\nratios (ESI-HRMS) and diagnostic ions for two families of suspected monoaromatic\nacids (GC × GC-TOF/MS). The resemblance between the AEO profiles from OSPW and from 6 groundwater samples adjacent to two tailings ponds implies a common source, supporting the use of these complimentary analyses for source identification. These samples included two of upward flowing groundwater collected <1 m beneath the Athabasca River, suggesting OSPW-affected groundwater is reaching the river system.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.007
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: Not applicable
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.485
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.007
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.107
GPT teacher head0.361
Teacher spread0.254 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it