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Record W6966476133 · doi:10.48336/eadv-tm79

Dipolar-depletion: study of a field-tunable colloid-polymer system

2023· article· en· W6966476133 on OpenAlexaff

Bibliographic record

VenueMemorial University Research Repository (Memorial University) · 2023
Typearticle
Languageen
FieldChemistry
TopicElectrostatics and Colloid Interactions
Canadian institutionsMemorial University of Newfoundland
Fundersnot available
KeywordsPhase diagramPolymerDipoleElectric fieldColloidPolarization (electrochemistry)PolarRelaxation (psychology)

Abstract

fetched live from OpenAlex

Colloidal gels are an important class of materials with mesoscale building blocks, and they have wide-ranging applications, from water purification to cement to biotechnology. However, the formation of colloidal gels is beset by inadequate control over phase behaviour and slow aging kinetics. In this work, we report on experiments that examine structure, structural relaxation and dynamics in colloid-polymer suspensions, with fine, tunable control: the concentration of non-adsorbing polymer controls the strength of a depletion attraction, and an external electric field induces dipolar interactions that are instantly switchable and tunable in strength. ßWith these switchable interactions, we have studied the “dipolar-depletion” phase diagram in real space via fluorescence confocal laser scanning microscopy. We show combining depletion with dipolar interactions, at lower polymer concentrations, lowers the field threshold for observing ordered sheet-like dipolar structures. At intermediate polymer concentrations, depletion-induced clusters suppress field-induced ordering. At high depletion strengths, we can create partially ordered gel states. We also quantitatively characterize the transition from reversible to irreversible structures, and use the cycling of the external field to accelerate aging in a gel-forming system. For processes that take months or years to study, such as the collapse of certain gels, such accelerated aging would prove extremely useful. In addition, we characterize our model system by measuring the Zeta potential and charge on the colloids that we use to study the phase diagram via both AC and DC microelectrophoresis. We compare AC and DC measurements and find that there is no electrode polarization effect in a partially polar solvent.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.438
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.003
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0010.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.024
GPT teacher head0.267
Teacher spread0.243 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2023
Admission routes1
Has abstractyes

Explore more

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