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Record W7110017192 · doi:10.1590/s2175-97902025e24597

Clobetasol brazilian pilot study: the vasoconstrictor assay over time

2025· article· en· W7110017192 on OpenAlexaff

Bibliographic record

VenueBrazilian Journal of Pharmaceutical Sciences · 2025
Typearticle
Languageen
FieldPharmacology, Toxicology and Pharmaceutics
TopicAdvancements in Transdermal Drug Delivery
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsBioequivalencePopulationDrugGold standard (test)ED50

Abstract

fetched live from OpenAlex

The vasoconstrictor assay (VCA) has been internationally recognized as a reliable method to evaluate the bioequivalence of topical corticosteroids. The FDA has recommended its use since 1995 and ANVISA began to require this assay in 2022 (RDC no. 742/22). The objective of this study was to compare results from two VCA pilot studies, using two Konika Minolta® instruments and two different estimation methods. The Emax and ED50 parameters were obtained using a nonlinear mixed effect model and least squares fit using a Gauss-Newton algorithm. Regardless of the equipment or the fitting methods, similar Emax and ED50 were obtained. However, both parameters were different when comparing the assays performed from different batches of the same reference list drug (RLD) and procedures from the different guides. Added to this, the tests were carried out at different times and in different seasons. In the VCA pilot study, estimating the ED50 is essential to determine the D1 and D2 (shorter and longer dose duration reference standard calibrator) to be used in the pivotal bioequivalence study. The diversity of the Brazilian population and the lack of experience to perform the procedure represent major challenges for the implementation of this test.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.006
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.776
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0060.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0010.002
Scholarly communication0.0000.001
Open science0.0020.000
Research integrity0.0000.002
Insufficient payload (model declined to judge)0.0080.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.113
GPT teacher head0.469
Teacher spread0.357 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designNot applicable
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes1
Has abstractyes

Explore more

Same venueBrazilian Journal of Pharmaceutical SciencesSame topicAdvancements in Transdermal Drug DeliveryFrench-language works237,207