Determination of lead in wax crayon using flame atomic absorption spectrometry / Suhailey binti Mohd Noor
Bibliographic record
Abstract
The method for the determination of lead in wax crayon by Flame Atomic Absorption Spectrometry was adopted from Health Canada Safety Program (HCSP), Product Safety Laboratory, ‘Determination of Total Lead in Wax Crayon by Closed Vessel Micowave Digestion’ and verified. The parameter of method verification such as accuracy, precision, limit of detection, limit of quantitation and linearity were studied. Three colours from 10 boxes of wax crayon samples were analysed. Microwave digestion method was used to extract the lead prior to analysis. The concentration of lead in red, blue and orange colour wax crayon was 25.23 ± 3.26 mg kg-1, 21.21 ± 3.44 mg kg-1 and 32.15 ± 0.35 mg kg-1 respectively. Our results also indicate that, there is no significant different in lead content between blue and red colour wax crayon. However, there is significant different in amount of lead in orange colour compared to blue and red colour wax crayon. Previous study had estimated that a greater than 15 ug/day intake of available lead could cause a previously normal child to exceed a 10 ug/dl blood level which gave toxic effect to children.
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How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.001 | 0.001 |
| Science and technology studies | 0.001 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.006 | 0.002 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".