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Record W7117293324 · doi:10.1021/jacs.5c15656

Cation-Ordering-Driven Design of Superionic Lithium Halospinels

2025· article· en· W7117293324 on OpenAlexaff
Yubo Wang, Manas Likhit Holekevi Chandrappa, Issei Otani, A. Dominic Fortes, Christopher Howard, Mengyang Cui, Balachandran Radhakrishnan, Lanting Qian, Linda F. Nazar

Bibliographic record

VenueJournal of the American Chemical Society · 2025
Typearticle
Languageen
FieldEngineering
TopicAdvanced Battery Materials and Technologies
Canadian institutionsUniversity of Waterloo
FundersScience and Technology Facilities CouncilNissan North America
KeywordsElectrolyteIonic conductivityLithium (medication)Fast ion conductorIonic bondingConductivityDensity functional theoryWork (physics)

Abstract

fetched live from OpenAlex

Reducing the material cost of inorganic solid-state electrolytes is crucial to advancing all-solid-state batteries (ASSBs) for next-generation energy storage applications. The halospinel Li 2 Sc 2/3 Cl 4 solid electrolyte (SE) possesses a high ionic conductivity of 1.5 mS cm –1 and good cycling stability up to 4.6 V. However, the high cost of Sc limits its practical application. In this study, we combine M3GNET universal machine learning interatomic potential (UMLIP) and density functional theory (DFT) for efficient screening of lower-cost cation-substituted halospinel compositions for synthesis. As a cost-mitigation strategy, predicted Mg 2+ -, Al 3+ -, and Zr 4+ -substituted Li 2 Sc 2/3 Cl 4 spinels with substitution fractions ranging from 20.9% to 37.5% were experimentally synthesized with only minor impurities, achieving room-temperature ionic conductivities as high as 1.85 mS cm –1 . Substitution of Fe 3+ was also achieved, albeit with a 7% Fe 2+ impurity. Molecular dynamics simulations (MD) using highly accurate moment tensor potentials (MTPs) indicate that Li + /Sc 3+ /M n+ ordering plays a crucial role in determining the conductivity of disordered substituted compositions. ASSBs operating at 3.8 mAh cm –2 capacity with Li 1.75 Sc 0.416 Zr 0.25 Cl 4 at a high current density of 2 mA cm –2 exhibited 80% of the capacity of more moderately loaded ASSBs cycled at a low rate. This work provides a foundational methodology for predicting the thermodynamic stability and ion transport of disordered lithium solid electrolytes and accelerating the discovery of novel materials for a range of applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.039
Threshold uncertainty score0.240

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.232
Teacher spread0.224 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2025
Admission routes1
Has abstractyes

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