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Record W7132942866

Assessment of strategies for measuring Cl-36 in natural samples

2004· dissertation· W7132942866 on OpenAlexaboutno aff
Jonathan P. Doupé

Bibliographic record

VenueTSpace · 2004
Typedissertation
Language
FieldEarth and Planetary Sciences
TopicGroundwater and Isotope Geochemistry
Canadian institutionsnot available
Fundersnot available
KeywordsAccelerator mass spectrometryIonIsobarArgonMass spectrometryIon sourceIsotopeIon beamAnalytical Chemistry (journal)
DOInot available

Abstract

fetched live from OpenAlex

The cosmogenic isotope 36Cl (half-life of 3.01 x 105 years) has been applied to problems in hydrogeology and surface exposure dating for a number of years. However its measurement in natural samples is complicated by its low abundance with respect to the stable isotopes of chlorine (36Cl/Cl = 10-10 to 10-16), and the presence of the isobar 36S (0.02% of S). Conventional Accelerator Mass Spectrometry (AMS) techniques for measuring 36Cl require tandem accelerators of 5 MV or larger. Only these machines can accelerate the 36Sn+ ions to high enough energies for them to be separated in gas-filled magnets, or in dE/dx analysis in the final detector. The present work investigates the possibility of 36Cl analysis on smaller, more economical machines. It is demonstrated that 36Ar3+ and 36S3+ ions, generated from argon and SF6 gas within the 2 MV tandem accelerator at the University of Toronto, will not preclude 36Cl measurements. A gas ion source was developed in which Cl- ions are created when a negative ion beam transfers its charge to the gas ICl, and the Cl- ions are then extracted. The efficiency of Cl- generation was about 20% for a Cu- beam. Because of the instability of sulphur iodide (S2I2) at room temperature, and the resonant charge transfer reaction to ICl, this gas source should discriminate against 36S. It was also shown that in the collision of S - and Cl- ions with NO2 gas at about one milliTorr pressure, the S- was attenuated by about two orders of magnitude relative to the Cl-. Finally, the 25 MV Holifield accelerator at Oak Ridge, Tennessee was used to measure 36Cl with the completely stripped 36Cl 17+ ion. Because the completely stripped sulphur species has a charge of 16+, it was possible to separate this isobar from 36Cl in a magnet. These measurements detected 36Cl in seawater for the first time, and showed, unexpectedly, that the 36Cl/Cl ratio varies in the world ocean.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.004
metaresearch head score (Gemma)0.004
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.023

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0040.004
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.035
GPT teacher head0.313
Teacher spread0.278 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2004
Admission routes1
Has abstractyes

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