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Record W2053991148 · doi:10.1021/ja9939688

Influence of β-Sheet Structure on the Susceptibility of Proteins to Backbone Oxidative Damage:  Preference for <sup>α</sup>C-Centered Radical Formation at Glycine Residues of Antiparallel β-Sheets

2000· article· en· W2053991148 on OpenAlexaff
Arvi Rauk, David A. Armstrong

Bibliographic record

VenueJournal of the American Chemical Society · 2000
Typearticle
Languageen
FieldChemistry
TopicFree Radicals and Antioxidants
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsChemistryAntiparallel (mathematics)RadicalBeta sheetProtein secondary structureCrystallographyRandom coilHydrogen bondStereochemistryProtein structureCircular dichroismMoleculeOrganic chemistryBiochemistry

Abstract

fetched live from OpenAlex

Ab initio calculations at the B3LYP/6-31G(d) level of theory were carried out on selected cyclic hydrogen-bonded (H-bonded) dimers of glycine and alanine as models for β-sheets and on the α C-centered radicals derived from them. The structures mirrored the cycles found in the H-bonded network of parallel and antiparallel β-sheet secondary structure, and were otimized both with and without enforcement of constraints on the Φ,Ψ torsion angles. Transition structures for the migration of an H atom from an α C site to another α C site or to an S atom were located. It was found that the presence of a H-bonded strand of a β-sheet has little effect on the α C−H bond dissociation enthalpy (BDE) of glycine but raises the BDE of other residues by a significant amount. The parallel β-sheet structure and Φ,Ψ angles lead to a significant increase in BDE, relative to the random coil structure, due to loss of captodative stabilization. The antiparallel β-sheet structure and Φ,Ψ angles do not lead to a significant increase in BDE. All residues incorporated in β-sheet secondary structure, with the exception of glycine, are protected from oxidative damage because the α C−H bond is internal to the sheet and inaccessible to oxidizing radicals. Glycine is susceptible to oxidative damage because it has a second α C−H bond which is exposed. Among residues in secondary structures, only glycine is susceptible to damage by weak oxidants such as thiyl radicals and superoxide, provided it is in an antiparallel β-sheet. Radical damage may propagate readily from one strand to another above the β-sheet, but not within the β-sheet. β-Sheet structure narrows the difference between the glycyl α C−H BDE and S−H BDE and facilitates interstrand H atom transfer between the glycyl α C site and the S atom of cysteine.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.014
Threshold uncertainty score0.483

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.253
Teacher spread0.236 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations57
Published2000
Admission routes1
Has abstractyes

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