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Record W2160953463 · doi:10.1096/fj.09-143743

New potent dual inhibitors of CK2 and Pim kinases: discovery and structural insights

2010· article· en· W2160953463 on OpenAlexfundno aff
Miriam López‐Ramos, Renaud Prudent, Virginie Moucadel, Céline F Sautel, Caroline Barette, Laurence Lafanéchère, Liliane Mouawad, David S. Grierson, Frédéric Schmidt, Jean‐Claude Florent, P. Filippakopoulos, Alex N. Bullock, Stefan Knapp, Jean‐Baptiste Reise, Claude Cochet

Bibliographic record

VenueThe FASEB Journal · 2010
Typearticle
Languageen
FieldMedicine
TopicCancer Mechanisms and Therapy
Canadian institutionsnot available
FundersCollege of Natural Resources and Sciences, Humboldt State UniversityKnut och Alice Wallenbergs StiftelseOntario Ministry of Community and Social ServicesGlaxoSmithKline AustraliaInstitut National Du CancerKarolinska InstitutetLigue Genevoise Contre le CancerInstitut National de la Santé et de la Recherche MédicaleCalifornia Earthquake AuthorityGenome CanadaFondation pour la Recherche MédicaleHamner Institutes for Health SciencesCanadian Foundation for AIDS ResearchOntario Innovation TrustMerck
KeywordsKinomeKinaseThreonineBiochemistryCasein kinase 1SerineCasein kinase 2ChemistryBiologyPhosphorylationProtein kinase ACyclin-dependent kinase 2

Abstract

fetched live from OpenAlex

ABSTRACT Protein kinase casein kinase 2 (CK2) is a serine/threonine kinase with evidence of implication in growth dysregulation and apoptosis resistance, making it a relevant target for cancer therapy. Several CK2 inhibitors have been developed showing variable efficiency, emphasizing the need to expand the chemical diversity of those inhibitors. We report the identification and characterization of 2,8‐difurandicarboxylic acid derivatives as a new class of nanomolar ATP‐competitive inhibitors. Selectivity profiling pointed out proviral insertion Moloney virus kinases (Pim kinases) as the only other kinases that are significantly inhibited. By combining structure‐activity relationship analysis with structural determination, we were able to determine the binding mode of these inhibitors for both kinases and to explain their strong inhibitory potency. Essential chemical features necessary for activity on both kinases were then identified. The described compounds are not cell permeable: however, they could provide a lead for developing novel inhibitors usable also in vivo . Given the similar but not redundant pathophysiological functions of CK2 and Pim family members, such inhibitors would provide new attractive leads for targeted cancer therapy. This work highlights that 2 functionally related kinases from different kinome branches display exquisite sensitivity to a common inhibitor.—López‐Ramos, M., Prudent, R., Moucadel, V., Sautel, C. F., Barette, C., Lafanechère, L., Mouawad, L., Grierson, D., Schmidt, F., Florent, J.‐C., Filippakopoulos, P., Bullock, A. N., Knapp, S., Reiser, J.‐B., Cochet, C. New potent dual inhibitors of CK2 and Pim kinases: discovery and structural insights. FASEB J . 24, 3171–3185 (2010). www.fasebj.org

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0020.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.239
Teacher spread0.231 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations64
Published2010
Admission routes1
Has abstractyes

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