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Record W2583866577 · doi:10.1002/celc.201700059

Probing Excimers of Pt(II) Compounds with Phenyl‐1,2,3‐Triazolyl and Pyridyl‐1,2,4‐Triazolyl Chelate Ligands by Means of Electrochemiluminescence

2017· article· en· W2583866577 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueChemElectroChem · 2017
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicAdvanced biosensing and bioanalysis techniques
Canadian institutionsQueen's UniversityWestern University
FundersNatural Sciences and Engineering Research Council of CanadaWestern University
KeywordsElectrochemiluminescencePhosphorescenceChemistryChemiluminescenceAmmonium persulfatePhotochemistryChelationPersulfateMethylamineExcited stateLigand (biochemistry)ElectrochemistryFluorescenceInorganic chemistryCatalysisPhysical chemistryOrganic chemistryElectrode

Abstract

fetched live from OpenAlex

Abstract Pt(II) complexes are well known for their excellent phosphorescence properties. Here, we report the results of an electrochemical and electrochemiluminescence (or electrogenerated chemiluminescence, ECL) study of two Pt complexes with phenyl‐1,2,3‐triazolyl and pyridyl‐1,2,4‐triazolyl chelate ligands to explore their effectiveness as ECL luminophores. The two Pt complexes with the two substituents CF 3 and t‐Bu on the pyridyl‐1,2,4‐triazolyl ligand (Pt1 and Pt2) were purposely chosen to see the structure and ECL correlations. It was discovered that excimers, the excited states of analyte dimers, contributed mainly to the ECL production. These two complexes exhibited weak ECL efficiencies following the annihilation mechanism. However, ECL was enhanced with co‐reactants such as tri‐ n ‐propylamine for Pt1 and ammonium persulfate for Pt2. Spooling ECL spectroscopy was utilized to gain analytical insight into light emission mechanisms. It is shown that excimers were probed easily by means of ECL.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.238
Teacher spread0.232 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it