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Record W2955588652

Synthetic analogs of the marine natural product hemiasterlin: Optimization and discovery of E7974, a novel and potent antitumor agent

2005· article· en· W2955588652 on OpenAlexaboutno aff
James J. Kowalczyk, Shawn Schiller, Mark R. Spyvee, Yang Hu, Boris M. Seletsky, Christina J. Shaffer, Veronique Marceau, Ye Yao, Galina Kuznetsov, Karen TenDyke, Diana Liu, Cheryl A. Rowell, Bruce A. Littlefield, Edward M. Suh

Bibliographic record

VenueCancer Research · 2005
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicMarine Sponges and Natural Products
Canadian institutionsnot available
Fundersnot available
KeywordsChemistryStereochemistryQuantitative structure–activity relationshipNatural productTopoisomeraseSteric effectsCombinatorial chemistryDNABiochemistry
DOInot available

Abstract

fetched live from OpenAlex

1213 A series of 13 anthrapyrazole (AP) compounds that were analogs of piroxantrone and losoxantrone were synthesized. Three-dimensional quantitative structure-activity analyses (3D-QSAR) were carried out on the AP compounds using comparative molecular field analysis (CoMFA) and comparative molecular similarity index analysis (CoMSIA) in order to determine the factors affecting the cell growth inhibitory (CHO, DZR, K562 and K/VP.5 cells), DNA binding (ΔTm) and inhibition of DNA topoisomerase II decatenation catalytic activity. Conformational analysis of all analogs was first performed with the CONFORT module implemented in SYBYL to identify the global minimum energy conformation. The most active compound, AP10, was then used as the template molecule. Steric and electrostatic fields were determined in CoMFA and three additional fields (hydrophobic, hydrogen donor and hydrogen acceptor) were determined in CoMSIA. Both CoMFA and CoMSIA analysis of the biological properties yielded statistically significant models upon partial least squares analysis. The information obtained from CoMFA and CoMSIA 3D-contour maps is to be used to predict the activity of new anthrapyrazoles with increased activity. Support: CIHR and a Canada Research Chair in Drug Development

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.314
Teacher spread0.292 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2005
Admission routes1
Has abstractyes

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Same venueCancer ResearchSame topicMarine Sponges and Natural ProductsFrench-language works237,207