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Record W4280618815 · doi:10.1016/j.ceja.2022.100322

Role of redox reactions involving interfacial oxygen migration in ignition of nanolayered Al/a-Al2O /CuO energetic composite

2022· article· en· W4280618815 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueChemical Engineering Journal Advances · 2022
Typearticle
Languageen
FieldEngineering
TopicEnergetic Materials and Combustion
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsThermiteExothermic reactionMaterials scienceRedoxMetastabilityOxidizing agentChemical physicsIgnition systemDiffusionAmorphous solidChemical engineeringChemical kineticsKineticsChemical reactionActivation energyThermodynamicsPhysical chemistryAluminiumComposite materialChemistryMetallurgyCrystallographyOrganic chemistry

Abstract

fetched live from OpenAlex

Thermite reactions of nanoparticles involve complex interplays between phase transition and heterogeneous atomic diffusion, especially at the early stage where the temperatures are relatively low and the systems remain as condensed phases. Moderate-temperature redox reactions among these condensed-phase reactants are investigated for a nanostructured 2.2 nm thick Al/CuO multilayer using ab initio molecular dynamics simulations. In order to achieve metastability, one amorphous alumina (a-Al2Ox) nanolayer of 0.6 nm is created between the Al and CuO layers. While the simulation is capable of predicting the energetic behaviors of the composite, focus is placed on investigating the species migration and reaction kinetics near these two interfaces, i.e., Al/a-Al2Ox and a-Al2Ox/CuyO. A set of redox reactions, possessing low activation barriers and a high exothermicity, are found to be critical to initiate the overall thermite reaction through generating localized hot spots within the a-Al2Ox layer and at its two interfaces, which has not been reported before. Driven by this exothermic process, migration of reactive species is promoted in condensed phases and a rate-limiting energy barrier (∼208.8 kJ•mol−1) at the Al/a-Al2Ox interface is overcome, which subsequently triggers a massive oxygen diffusion throughout the multilayer. Examination on chemical kinetics further reveals that the redox capacity of the a-Al2Ox layer determines the solid-state species migration during the ignition stage of the thermite reaction through two pathways: (1) the low-barrier and exothermic O migration in the a-Al2Ox layer and at the corresponding interfaces; (2) the migration-induced processes including decomposition of the CuO layer and melting of the Al. Contributions of the new simulation results to the existing reaction mechanisms are clarified.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.332
Threshold uncertainty score0.516

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.183
Teacher spread0.180 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it