MétaCan
Menu
Back to cohort
Record W4390661799 · doi:10.1002/ejoc.202301205

C‐Centered radical intermediates for C(sp<sup>3</sup>)‐H bonds functionalization: An emerging approach towards alkyl thiocyanates

2024· article· en· W4390661799 on OpenAlex
Floris Buttard, Jordan Vigier, H. Lebel, Tatiana Besset

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueEuropean Journal of Organic Chemistry · 2024
Typearticle
Languageen
FieldChemistry
TopicSulfur-Based Synthesis Techniques
Canadian institutionsUniversité de MontréalCentre in Green Chemistry and Catalysis
FundersInstitut Carnot Santé AnimaleCanada Foundation for InnovationUniversité de RouenRégion NormandieUniversité de MontréalCentre National de la Recherche ScientifiqueAgence Nationale de la RechercheNatural Sciences and Engineering Research Council of CanadaEuropean Regional Development FundCentre in Green Chemistry and CatalysisEuropean CommissionIndian National Science Academy
KeywordsChemistrySurface modificationMoietyCombinatorial chemistryAlkylThiocyanateMoleculeOrganic synthesisOrganic chemistryCatalysis

Abstract

fetched live from OpenAlex

Abstract Organic thiocyanates are an important class of compounds because they are present in several bioactive molecules and can be used as key synthetic intermediates to access biorelevant sulfur‐containing scaffolds. Although the chemistry of organothiocyanates has been studied for decades, a recent resurgence of interest in the field has led to major advances in the synthesis of new molecules bearing a thiocyanate moiety. An emerging and powerful strategy consists in the selective functionalization of C(sp 3 )‐H bonds through the formation of a key C‐centered radical intermediate. This review highlights the recent work that has been reported to access novel alkylthiocyanate scaffolds through this promising approach.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.065
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0050.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.024
GPT teacher head0.259
Teacher spread0.235 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it